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... ............................................................................................. 140 5.7.1 - Synthesis general................................................................................................ 140 5.8 - Acknowledgments ................................................................................................... 142 5.9 - References ............................................................................................................... 143 Page Chapter 6: Synthesis... of Royal Society London A, 1852, 142, 463-562. [2] Czarnik, A.W.; Accounts of... (C4), 127.87 (C3 and C5), 148.35 (C2), 148.70... (C4), 127.41 (2 — (C3 and C5), 127.56 (2— C4’), 128.62... C6’), 129.04 (2— (C3’ and C5’)), 147.79 (C2), 148.91....09 (2×C3’and 2×C5’), 127.57 (C3 and C5), 127.96 (2×C4... (CH3), 52.94 (αC), 119.36 (C5), 125.46 (C1), 126.15... (αC), 80.27 (C(CH3)3), 120.09 (C5), 125.25 (C2), 128.62... (αC), 80.11 (C(CH3)3), 115.30 (C5), 117.33 (C2), 119.89...)3), 114.99 (C2), 116.54 (C5), 127.56 (C1), 127.99...’ or C5’), 132.59 (C3’ or C5’), 134.98 (C3), 142.73 (C2...), 115.71 (C6’), 116.33 (C5), 127.71 (C1), 129.76...), 135.12 (C3), 135.79 (C5’), 144.76 (C4’), 149.79....97 (C3’), 130.31 (C5’), 132.79 (C5), 142.28 (C3a), 149.59....73 (C3’), 130.84 (C5’), 133.24 (C5), 141.26 (C3a), 149....97 (C3’), 130.31 (C5’), 133.85 (C5), 142.33 (C3a), 149.49... (β CH2), 53.01 (αC), 109.92 (C5’), 119.40 (C7), 126.57...), 131.38 (C3’), 132.34 (C5), 141.36 (C3a), 151.70....90 (C2), 133.34 (C5), 135.93 (C5’), 141.18 (C3a), 145....06 (C4), 132.55 (C5), 135.41 (C5’), 141.34 (C3a), 145... .............................................................................................. 140 5.7.1 - Synthesis general ............................................................................................... 140 5.8 - Acknowledgments ................................................................................................... 142 5.9 - References ............................................................................................................... 143 129 Chapter 5 5.1 - Graphical...’), 125.18 (C3’’), 126.02 (C5’’), 127.61 (C1), 128.21 (C4’’), 129.49 (C5), 133.51 (C4’), 134.95... (C2’ or C2’’), 141.09 (C5’), 142.88 (C2’ or C2’’), 149...), 124.43 (C4’), 125.07 (C5’’), 125.90 (C3’’), 126.31... (C3’), 132.85 (C5), 136.19 (C2’’), 142.30 (C5’), 142.35 (C3a), 149...), 124.47 (C4’), 125.13 (C5’’), 125.79 (C3’’), 126.58... (C3’), 133.01 (C5), 136.10 (C2’’), 142.20 (C5’), 142.03 (C3a), 149...), 124.41 (C4’), 125.24 (C5’’), 125.80 (C3’’), 126.57....41 (C5), 136.35 (C2’’), 141.03 (C3a), 142.33 (C5’), 151.62... for derivatives 4a-c and 6a-c. 142 13 C NMR, MS and HRMS... (C2), 128.97 (C3’’ and C5’’), 130.51 (C3’), 131.22 (C5’), 133.08 (C5), 138.12 (C1’’), 141... (C6), 128.37 (C3’’ and C5’’), 128.62 (C4’), 128.91....40 (C3’), 131.83 (C5’), 135.22 (C5), 138.24 (C1’’), 141... C6’’), 128.97 (C3’’ and C5’’), 137.84 (C1’’), 155.28... C6’’), 128.85 (C3’’ and C5’’), 137.64 (C1’’), 155.67... (0.14 g, 42 %), melting point = 140-142 ºC, C33H38N4O7S2, FW= 666.8. Elemental Analysis....80 (C3’), 131.01 (C5’), 133.10 (C5), 137.91 (C1’’), 141...), 120.5 (C4 BOT), 123.03 (C5 Trp), 123.62 (C3’ ZNO2....77 (C 4’’), 128.27 (C3’’ and C5’’), 128.56 (C4’), 128.64....31 (C3’), 131.76 (C5’), 134.77 (C5 BOT), 135.13 (C7a... (C1’’), 141.28 (C3a BOT), 142.97 (C1’ ZNO2), 147.23...), 125.21 (C4’), 125.89 (C5’’), 125.96 (C3’’), 126.18...’’), 128.67 (C3’), 131.68 (C5), 135.00 (C2’’), 141.63 (C5’), 141.69 (C3a), 149.26 (...), 125.47 (C4’), 125.10 (C5’’), 125.93 (C3’’), 126.38... (C4’’),128.56 (C3’’’ and C5’’’), 128.89 (C2’’’ and C6....25 (C5), 136.24 (C2’’), 137.60 (C1’’’), 142.33 (C5’), 142.47 (C3a... (C6), 127.36 (C5’’), 128.28 (C3’’’ and C5’’’), 128.75 (C4...’’’), 131.48 (C3’), 134.16 (C5), 135.15 (C2’’), 138.35 (C1’’’), 141.50 (C5’), 141.54 (C3a), 148.89...



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... lediglich in ihren Substituenten am C5 des Pyrrolidin-2,4-dionsystems (H oder Methyl... 141 tButylpropionat Propyl Heptyl 26 142 Propansäure Ethyl Pentadecyl 23... N C6H13 O 122 O OH N C14H29 O O OH 142 57 Spezieller Teil a Angegebenen sind...-Probe) wurde somit die Substanz 142 (Tabelle 4-4) ausgewählt. Überraschenderweise erwies... H 29 N O O a) HO N O OH C 14H 29 O 142 147 O HN H NH H b) O S N H O HN H H H S O O O NH... per Western-Blot erreicht werden.[142] Des Weiteren sollte die Bindung....8 (C4), 101.8 13 (C3), 57.9 (C5), 33.0 (C1’), 32.1 (C7), 29....7 (C4), 101.8 13 (C3), 57.9 (C5), 32.8 (C1’), 32.1 (C7), 29....8 (C4), 101.8 13 (C3), 57.9 (C5), 33.1 (C1’), 32.1 (C7), 30....8 (C4), 101.8 13 (C3), 57.9 (C5), 33.0 (C1’), 32.1 (C7), 29....8 (C4), 101.8 13 (C3), 57.9 (C5), 32.8 (C1’), 32.1 (C7), 29....5 (C4), 101.6 13 (C3), 57.6 (C5), 32.6 (C7), 31.8- 29.1 (C8....2 (C4), 102.2 13 (C3), 57.6 (C5), 28.3 (C1’), 19.4 (C7). MALDI....2 (C4), 100.3 13 (C3), 57.9 (C5), 31.2 (C 1’), 28.6 (C7), 18.9 (2CH3...), 116.2 (C10), 102.1 (C3), 57.9 (C5), 32.1 (C1’), 29.8 (C7), 28....), 126.6 (ar.), 102.1 (C3), 57.9 (C5), 34.5 (benz.), 31.9 (benz.), 28....), 114.6 (ar.), 102.6 (C3), 55.5 (C5), 55.1 (OCH3), 45.0 (benz.), 19....), 102.8 (C3), 98.8 (ar.), 56.0 (C5), 55.6 (OCH3), 55.6 (OCH3), 40....0 (CH2=CH2), 101.8 (C3), 57.9 (C5), 32.8 (C1’), 32.0 (C7), 29....), 55.9 (OCH3), 55.6 (OCH3), 55.6 (C5), 40.2 (benzyl.), 33.0 (C1’), 32....1 (C4), 100.7 13 (C3), 62.9 (C5), 32.8 (C1’’), 32.1 (C7), 29....8 (C4), 102.3 13 (C3), 70.4 (C5), 35.8 (C1’’), 32.7 (CHCH2CH3), 32...), 130.0 (C12), 101.8 (C3), 57.9 (C5), 32.8 (C1’’), 32.0 (C7), 29....9 (C4), 102.1 13 (C3), 71.6 (C5), 32.7 (C1’’), 32.1 (C7), 29...)3), 101.5 (C3), 81.0 (C(CH3)3), 62.9 (C5), 34.4 (C1’’), 33.0 (C7, C2...), 101.5 (C3), 81.0 (C(CH3)3), 62.9 (C5), 34.4 (C1’’), 32.7 (C7, C2....), 101.6 (C3), 81.0 (C(CH3)3), 63.0 (C5), 41.5 (C1’’), 32.9 (C7, C2....), 123.5 (ar.), 101.3 (C3), 62.6 (C5), 41.7 (C1’’), 33.0 (C7, C2...), 101.4 (C3), 81.0 (C(CH3)3), 63.2 (C5), 41.1 (C1’’), 33.0 (C7), 32...), 101.4 (C3), 81.0 (C(CH3)3), 63.2 (C5), 41.1 (C1’’), 34.0 (C7), 31....5 13 (CH2COOH), 101.4 (C3), 62.6 (C5), 34.4 (C1’’), 32.8 (C7, C2....1 (C4), 171.8 13 (COOtbutyl), 136.7 (C5’’), 135.0 (C2’’), 128.6 (C3’’), 123...’’), 101.3 (C3), 80.7(C(CH3)3), 62.9 (C5), 41.1 (C1’’), 32.7 (C6’’), 32....5 (C4), 173.4 13 (COOH), 137.1 (C5’’), 135.5 (C2’’), 128.8 (C3’’), 123.1 (C4’’), 101.4 (C3), 62.9 (C5), 41.5 (C1’’), 33.0 (C6’’), 32...), 100.8 (C3), 80.3 (C(CH3)3), 62.2 (C5), 33.7 (C1’’), 32.3 (C7), 31..., CHCl3) (S,Z)-3-(1-Hydroxyhexadecyliden)-5-propanoat-1-ethylpyrrolidin-2,4-dion (142) (S,Z)-3-(1-Hydroxyhexadecyliden)-5-tert-butyl-3-propanoat-1-ethylpyrrolidin....5 13 (COOH), 101.4 (C3), 62.6 (C5), 34.5 (C1’’), 33.1 (C7, C2... 98.7 (ar.), 80.9 (C(CH3)3), 63.7 (C5), 55.6 (OCH3), 55.6 (OCH3), 38....), 101.5 (C3), 79.1 (ar.), 68.2 (C5), 35.1 (C1’’), 33.1 (benz.), 32....), 100.0 (C3), 79.0 (C(CH3)3.), 64.9 (C5), 44.0 (benz.), 41.2 (CH), 35....), 100.0 (C3), 78.7 (C(CH3)3), 64.8 (C5), 43.9 (benz.), 41.0 (CH), 37....), 101.4 (C3), 78.7 (C(CH3)3), 64.9 (C5), 43.9 (benz.), 35.3 (benz.), 32....), 127.2 (ar.), 101.6 (C3), 64.8 (C5), 35.7 (C1’’), 34.8 (benz.), 32....), 110.0 (ar.), 100.2 (C3), 64.7 (C5), 41.0 (C1’’), 35.8 (C1’), 34....), 104.8 (C3), 98.7 (C(CH3)3) 64.2 (C5), 55.6 (OCH3), 55.6 (OCH3), 40...), 100.1 (C3), 81.0 (C(CH3)3), 62.9 (C5), 41.2 (CH und C3’), 34....), 100.8 (C3), 77.4 (C(CH3)3), 63.9 (C5), 43.7 (C3’), 41.6 (benz.), 33....4266 [α]20 = -27.0° (c = 0.26, CHCl3) 142 Experimenteller Teil (S,Z)-3-(1-Hydroxyhexadecyliden)-5-(tert-butoxymethyl....7 (CH ar.), 73.4 (C(CH3)3), 65.6 (C5), 59.5 (CH2Ot-butyl), 55.6 (OCH3....8 13 (C3), 73.6 (C(CH3)3), 65.7 (C5), 61.3 (CH2Ot-butyl), 35.4 (C1...), 98.5 (ar.), 73.4 (C(CH3)3), 65.4 (C5), 59.2 (CH2Otbutyl), 55.4 (OCH3), 55...), 99.8 (C3), 45.6 (C1’), 42.9 (C5), 37.9 (C6), 23.7 (CH3). LC....), 98.8 (C3), 55.6 (OCH3), 45.1 (C5), 43.1 (benz.), 38.1 (C6), 37....), 102.1(C3), 79.6 (C(CH3)3), 63.9 (C5), 43.6 (benz.), 40.3 (C3’), 28....), 114.1(ar.), 110.0 (C3), 63.0 (C5), 43.8 (benz.), 40.0 (C3’), 24....2 (C3), 59.3 (benzyl. C10), 55.8 (C5), 48.1(CH2 8), 44.2 (benzyl. C1....6 (C3), 138.4 (C4), 13 133.8 (C5), 131.7 (C6), 126.2 (7), 125.4 (C2...) = 196.1 (C1), 167.4 (C3), 149.7 (C5), 142.9 13 (C6), 137.9 (8), 137.1 (C9...), 168.3 (CH3OC(O)CH2), 13 150.8 (C5), 143.0 (C6), 139.8 (C8), 134...), 172.7 (C4), 150.5 13 (C8), 142.7 (C9), 139.6 (C11), 134.6 (C12....8 (C7), 103.4 (C3), 46.3 (C5), 41.7 (C5 Ketoform), 18.8 (C15), 12.6 (C9...) = 195.8 (C1), 166.6 (C3), 145.2 (C5), 139.7 13 (C6), 139.3 (C8...), 142.8 (CH), 130.1 (CH), 128.8 (CH), 120.1 (CH), 100.3 (C3), 57.4 (C5...) = 193.0 (C1), 164.3 (C3), 143.2 (C5), 143.0- 13 124.6 (CH Keto...), 120.6 (CH), 100.7 (C3), 57.8 (C5), 28.7 (NCH3), 19.0 (C13). LC...) = 196.1 (C1), 166.9 (C3), 145.2 (C5), 143.6- 13 124.3 (CH Keto...), 120.7 (CH), 100.7 (C3), 57.8 (C5), 28.7 (NCH3), 18.8 (C15). LC....4 (C3), 80.7-69.7 (OCH2CH2O), 61.9 (C5), 60.5 (NHCHCH2S), 51.6 (NHCHCHS), 52....2 (C3), 70.3-69.8 (OCH2CH2O), 62.8 (C5), 62.1 (NHCHCH2S), 60.6 (NHCHCHS), 55... Biology 2008, 10, 971-978. [142] O. George, B. K. Bryant, R. Chinnasamy, et al...



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... COMPLEXES D’AGI, D’AUI ET D’AUIII ................................... 142 1.-PROPRIÉTÉS DE LUMINESCENCE DES PROLIGANDS... de jonction alkyle (C3 et C5) et de la nature et... l’ultraviolet (< 400 nm) et le 142 Chapitre IV : propriétés photophysiques des... 0.1032 0.2099 0.0569 ∆ρmax/min/e Å-3 3.142 and -3.203 1.738 and -2.707...), 121.4 (1C, C3), 69.1 (1C, C5), 57.4 (2C, C4), 27.4 (2C...), 120.5 (1C, C3), 72.6 (1C, C5), 54.1 (1C, C4). MS (FAB... (1C, COMe), 18.42 (1C, C5). MS (ES+): m/z 155.2 [M + H+]+. [α]20D = + 3 (589... (1C, C4), 18.11 (1C, C5). MS (ES+): m/z 127.3 [M + H+]+. [α]20D = + 18...-), 138.1 (2C, CArTsO-), 137.4 (2C, C5), 128.5 (4C, CArTsO-), 125.9 (4C... MHz, DMSO-d6) δ: 138.4 (2C, C5), 125.6 (2C, C4), 123.0 (2C...), 68.6 (2C, C6), 59.7 (2C, C5), 58.5 (1C, C1), 28.1 (4C... (2C, CArTsO-), 136.17 (2C, C5), 128.54 (4C, CArTsO-), 125..., DMSO-d6) δ: 136.19 (2C, C5), 122.67 (2C, C3), 121... (2C, CArTsO-), 137.27 (2C, C5), 128.80 (4C, CAr), 128... (2C, CAr), 137.24 (2C, C5), 128.82 (4C, CAr), 128....9 (4C, CAr TsO ), 124.4 (2C, C5), 122.0 (2C, C4), 68.6 (2C... ), 122.7 (2C, C4), 121.6 (2C, C5), 64.3 (2C, C8), 58.6 (2C...), 125.9 (4C, CArTsO-), 123.7 (2C, C5), 122.4 (2C, C4), 188 Chapitre..., C3), 142.0 (1C, C1), 134.9 (2C, C6), 131.1 (2C, C5), 116.1 (2C...), 136.4 (2C, C6), 124.7 (2C, C5), 119.8 (2C, C4), 114.9 (2C...), 132.3 (2C, C1), 129.7 (2C, C5), 129.5 (2C, C4), 129.0 (2C..., DMSO-d6) δ: 181.3 (pseudod, 2C, C5), 146.3 (1C, CArTsO-), 138.1 (1C..., DMSO-d6) δ: 181.3 (dd, 2C, C5, J107C-Ag = 181.9 Hz and... MHz, DMSO-d6) δ: 181.4 (2C, C5), 124.6 (2C, C4), 120.7 (2C... (75 MHz, CD3CN) δ: 181.9 (2C, C5), 124.1 (2C, C4), 120.3 (2C... NMR (75 MHz, DMSO-d6) δ: 142.2 (2C, CAr),141.4 (2.2C, CArTsO... ), 122.1 (2C, C4), 120.1 (2C, C5), 65.4 (2C, C8), 59.8 (2C....2 (2C, C6),146.3 (3.8C, CArTsO-), 142.5 (2C, CAr), 138.1 (3.8C, CArTsO...-), 126.0 (4C, CAr), 124.7 (2C, C5), 121.5 (2C, C4), 72.9 (2C...), 144.3 (1C, C1), 124.6 (2C, C5), 120.0 (2C, C4), 114.4 (2C... (75 MHz, CD3CN) δ: 183.9 (2C, C5), 142.2 (3.2C, CArTsO-), 140.3 (3.2 C, CArTsO-), 128... (75 MHz, CD3CN) δ: 183.9 (2C, C5), 124.2 (2C, C4), 120.5 (2C...), 62.7 (1C, C1), 61.2 (2C, C5), 27.8 (2C, C7 or 8), 27...), 62.8 (1C, C1), 61.4 (2C, C5), 26.6 (2C, C7 or 8), 26...), 143.4 (1C, C1), 124.5 (2C, C5), 119.2 (2C, C4), 113.8 (2C... (75 MHz, CD3CN) δ: 183.1 (2C, C5), 141.1 (2C, CAr), 128.5 (4C... (63 MHz, CD3CN) δ: 183.1.0 (2C, C5), 121.4 (2C, C3), 119.5 (2C...), 63.8 (1C, C1), 60.2 (2C, C5), 27.3 (2C, C7 or 8), 26... (75 MHz, CD3CN) δ: 150.3 (2C, C5), 126.8 (2C, C4), 122.7 (2C...), 126.1 (2C, C2), 124.6 (2C, C5), 122.6 (2C, C4), 60.1 (2C... MHz, DMSO-d6) δ: 167.3 (1C, C5), 139.4 (1C, C1), 138.6 (1C... MHz, DMSO-d6) δ: 166.3 (1C, C5), 144.6 (1C, CAr), 138.6 (1C... 8 10 O 6 Formaldehyde water solution (36%, 0.142 g, 1.7 mmol) and glyoxal water solution... MHz, DMSO-d6) δ: 171.5 (1C, C5), 139.7 (1C, C1), 136.2 (1C...) δ: 164.1 (2C, C7), 138.7 (2C, C5), 138.2 (2C, CAr), 129.5 (4C...) δ: 165.4 (2C, C7), 139.1 (2C, C5), 138.1 (2C, CAr), 128.8 (4C...), 144.4 (2C, CAr), 138.1 (2C, C5), 128.8 (4C, CAr), 127.3 (2C...) δ: 167.1 (2C, C7), 138.6 (2C, C5), 137.1 (2C, CAr), 129.4 (4C...), 139.2 (2C, CAr), 137.1 (2C, C5), 128.8 (4C, CAr), 127.8 (4C... MHz, DMSO-d6) δ: 184.9 (2C, C5), 165.4 (2C, C7), 139.2 13... (63 MHz, DMSOd6) δ: 184.4 (2C, C5), 166.9 (2C, C7), 139.4 (2C...) δ: 166.6 (2C, C7), 162.1 (2C, C5), 148.4 (2C, CAr), 127.0 (4C...): δ = 169.7 (2C, C7), 162.1 (2C, C5), 142.2 (2C, CAr), 128.0 (4C, CAr...) δ: 166.6 (2C, C7), 161.8 (2C, C5), 148.1 (2C, CAr), 126.9 (4C...) δ: 170.2 (2C, C7), 161.2 (2C, C5), 142.1 (2C, CAr), 128.1 (4C, CAr...) δ: 174.1 (2C, C7), 165.2 (2C, C5), 143.3 (2C, CAr), 127.6 (4C...



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0.37/5
...-2 cells, Plant J., 2004, 40, 131-142. Copyright Wiley-Blackwell. Reproduced with... activity with pnitrophenylbutyrate (C4), valerate (C5) and caproate (C6) as that... divided into two orthogonal parts. 142 In a similar fashion, the structure... the following sections. 5.3.4.1 Brefeldin A Brefeldin A, 142 is a macrocyclic lactone that it....212 In cells treated with 142 protein secretion is inhibited at... the cell.214 O HO O H H HO 142 A. thaliana protoplasts were incubated with 100 μM 142 for 30 mins. Following treatment...), 153.1 (C7), 151.8 (QC), 125.4 (C5), 118.1 (C6), 117.9 (C4), 114...), 153.7 (C7), 152.2 (QC), 125.6 (C5), 118.2 (C6), 118.0 (C4), 114...), 153.2 (C7), 151.9 (QC), 125.3 (C5), 118.1 (C6), 117.7 (C4), 114....5 (C4’), 22.3 (C4-Me), 18.7 (C5’), 13.9 (C6’); m/z (ES+): 274.9 [M+H+]+ 191...), 153.5 (C7), 152.0 (QC), 125.4 (C5), 118.2 (C6), 117.8 (C4), 114...’-Me), 18.8 (C4-Me), 17.0 (C5’), 14.0 (C6’); m/z (ES+): 288.8 [M+H+]+ 192...), 153.2 (C7), 151.9 (QC), 125.4 (C5), 118.1 (C6), 117.7 (C4), 114...’), 32.2 (C3’), 31.3 (C4’), 29.1 (C5’), 18.8 (C4-Me), 18.6 (C4...), 152.7 (C7), 151.9 (QC), 125.6 (C5), 118.2 (C6), 117.9 (C4), 114...), 153.2 (C7), 152.0 (QC), 125.6 (C5), 118.2 (C6), 118.0 (C4), 114...), 153.2 (C7), 152.0 (QC), 125.6 (C5), 118.2 (C6), 118.0 (C4), 114...), 152.8 (C7), 152.2 (QC), 125.8 (C5), 118.3 (C6), 118.0 (C4), 114....7 (C2’), 29.5 (C4-Me), 18.9 (C5’), 9.8 (C6’); m/z (ES+): 312.08416 ([M+Na...), 152.7 (C7), 152.2 (QC), 125.9 (C5), 118.3 (C6), 118.0 (C4), 114....8 (C2’), 29.7 (C4-Me), 18.9 (C5’), 18.4 (C2’-Me), 9.9 (C6’); m/z (ES...), 125.5 (C3), 121.3 (C8), 118.2 (C5), 21.1 (Me); m/z (ES+): 187.1 [M+H]+ 2-naphthyl... 127.8 (C7 and C8), 126.7 (C5), 125.8 (C6), 121.3 (C3), 118...’), 142.1 (QC), 132.5 (C5’), 130.4 (C3’), 126.6 (C4’), 125.5 and 124.7 (C5 and... and C8a), 110.5 (C4 and C5), 81.9 (spiroC), 34.5 (C2’), 29... and C8a), 110.5 (C4 and C5), 81.9 (spiroC), 34.5 (C2’), 32... and C8a), 110.5 (C4 and C5), 81.8 (spiroC), 47.8 (C2’), 31...), 130.5 (C4), 120.5 (C3 and C5), 25.6 (tBu), 18.3 (QC), -4.3 (Me...), 122.6 (C4’), 120.3 (C3 and C5), 89.0 (C2’), 86.6 (C3’), 64... C6), 126.3 (C3’’ and C5’’), 120.7 (C3 and C5), 112.5 (C2’’ and...), 122.8 (ArC), 115.5 (C3 and C5), 89.9 (C2’), 85.6 (C3’), 64... and C6), 122.5 (C3 and C5), 21.3 (Me); m/z (ES+): 180.2 [M+H]+ 4-(1-hydroxy...), 122.7 (ArC), 122.1 (C3 and C5), 88.9 (C2’), 87.2 (C3’), 64....5 (ArC), 125.2 (C3’’ and C5’’), 122.1 (C3 and C5), 121.7 (ArC), 118...), 122.6 (C4’), 114.1 (C3 and C5), 89.0 (C2’), 86.6 (C3’), 64... and C6), 126.3 (C3” and C5”), 122.3 (C4’), 114.6 (C3 and C5), 112.5 (C2” and C6”), 86.8 (...), 127.5 (ArC), 113.9 (C3 and C5), 55.6 (OMe), 48.5 (C3’), 44...), 127.3 (ArC), 114.0 (C3 and C5), 87.8 (C2’), 86.8 (C3’), 55...), 128.6 (ArC), 114.6 (C3 and C5), 55.6 (OMe), 41.5 (C2’), 38...), 130.8 (C1), 116.4 (C3 and C5), 94.2 (CH2), 56.5 (CH3); m/z (ES....6 210 (ArC), 116.4 (C3 and C5), 94.6 (CH2), 89.0 (C3’), 86... and C6), 126.6 (C3” and C5”), 122.4 (C4’), 116.9 (C3 and C5), 112.9 (C2” and C6”), 94.5 (...), 144.3 (QC), 133.2 (QC), 132.0 (C5), 131.3 (ArC), 130.7 (ArC), 124...’), 132.0 (pyC), 131.8 (C3’ and C5’), 130.3 (C2’ and C6’), 121... MHz, CDCl3): 155.5 (C3 and C5), 143.3 (C1 and C7), 141...): 156.8 (C5 and C3), 148.5 (C4’), 142.7 (C7 and C1), 142.1 (C8), 138...’ and C6’), 124.5 (C3’ and C5’), 122.0 (C2 and C6), 14....9 (C2’), 156.5 (C3 and C5), 150.1 (C4’), 142.4 (C1 and C7), 136...’), 121.8 (C2 and C6), 117.0 (C5’), 106.6 (C3’), 56.8 (OMe), 15...), 135.1 (C4), 132.7 (C6), 126.3 (C5), 124.2 (C3), 122.3 (C1), 21... C7Me); δC (126 MHz, CDCl3): 152.6 (C5 and C3), 148.0 (C4’), 145...’ and C6’), 123.9 (C3’ and C5’), 120.4 (C2 and C6), 16... C7Me); δC (126 MHz, CDCl3): 154.9 (C5 and C3), 147.1 (C4’), 143...’ and C6’), 124.2 (C3’ and C5’), 120.6 (C2 and C6), 14... C7Me); δC (126 MHz, CDCl3): 155.1 (C5 and C3), 147.1 (C4’), 143...’ and C6’), 123.9 (C3’ and C5’), 120.4 (C2 and C6), 14... MHz, CDCl3): 154.7 (C3 and C5), 142.5 (C1 and C7), 141.4 (C8... MHz, CDCl3): 155.6 (C3 and C5), 142.1 (C1a and C7a), 141.9 (C1...); 177.0 (CHO), 161.0 (C4’), 159.9 (C5), 151.8 (C2), 127.1 (C2’ and...’), 121.9 (C1’), 114.6 (C3’ and C5’), 106.4 (furan C), 55.5 (OMe); m/z (ES...’), 124.1 (C1’), 123.3 (C5), 114.1 (C3’ and C5’), 96.3 (C6), 92.3 (C3...), 125.9 (C2’ and C6’), 124.6 (C5), 124.4 (C1’), 115.1 (C3’ and C5’), 96.4 (C6), 94.0 (C3), 55.9 (...’), 118.6 (QC), 114.7 (C3’ and C5’), 103.1 (C6), 94.2 (C3), 55..., s, Me); δC (126 MHz, CDCl3): 152.6 (C5 and C3), 148.0 (C4’), 145...’ and C6’), 123.9 (C3’ and C5’), 120.4 (C2 and C6), 16... Kuchitsu K., Plant J., 2004, 40, 131 – 142 109 Alberti S., Parks D. R. and Herzenberg.... Dispos., 1998, 26, 868 – 874 142 Mathijssen R. H. J. and van Schaik R. H. N., Eur... B. and Whiteman M., Br. J. Pharmacol., 2004, 142, 231 – 255 226 Khan N., Wilmot...



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0.17/5
... neutral glycine increases dramatically.141,142 In order to gain information...(1-MeC)(gly-N)]+ (a = NH3, NH2CH3).141,142 Thus, the results show that...)(gly-N)]+ (pKa = 2.8 and 2.5, respectively).141,142 44 3,75 3,70 3,65 δ / ppm..., the fully protected PNA pentamer c5 was assembled following a well-established... building blocks yielded resin-bound c5 (30). It was subsequently reacted... of building block 9 to immobilized c5 (30); a) HATU, DiPEA, b) cap reagent... Nterminal amino group of immobilized c5 proceeded almost quantitatively. An incomplete... coupling reaction of 9 with immobilized c5 (33) tr mass amount / % assignment... n.o. s, 7.32 s, 1.92 d, 3.64 m, 4.55 t, 2.15 T-C5 T-C6 T-CO(4) T-CO(2) 109.8 143... 50 A-C6 A-C2 A-C4 A-C8 A-C5 A-C9 48a 155.6 152.9 150... with A-C8 (1J), A-C4 (3J), A-C5 (3J), and A-C9 (3J). The... (3J), b: A-H2 / A-C6 (3J), c: A-H8 / A-C5 (3J), d: A-H8 / A-C4 (3J), e: T-H6... with A-C8 (1J), A-C4 (3J), A-C5 (3J), whereas A-H2 displays couplings... (3J), b: A-H2 / A-C6 (3J), c: A-H8 / A-C5 (3J), d: A-H8 / A-C4 (3J), e: T-H6... A-C5 T-C5 T-C6 T-CO(4) T-CO(2) 51b 157.7 155.6 148.9 142.6 121.6 110.5 142.9 174.4 158.9 Table 5 (continued) C1´ C2´ C3´ C4´ C5... a 4-hydroxymethylbenzoic acid linker. Assembly of c5 was performed using solutions of... (1/1, v/v), 2.5 ml. The immobilized fully protected c5 (30) was transferred into a syringe...), 144.5 (A-C8), 120.5 (A-C5), 51.1 (A-C9), 109.8 (T-C5), 143.0 (T-C6), 174.0 (T-CO....6 (A-C2), 148.9 (A-C4), 142.6 (A-C8), 121.5 (A-C5), 110.5 (T-C5), 142.9 (T-C6), 174.4 (T-CO(4)), 158...´), 73.6 (C3´), 87.3 (C4´), 63.8 (C5´); 195 Pt NMR (DMF-d7... 43 mit dem Deoxyoligonukleotid 46. 142 Die in Kapitel III beschriebene..., Chim. Acta, 1990, 168, 275. 142 F.J. Pesch, H. Preut, B. Lippert, Inorg, Chim...(PO3H)d(T2CTC2TC)-3´-OH}]+ 30* NH2-c5-gly-HMBA-PS 31 trans-[Pt(NH2CH3)2(CHMT)(NH2CH2CONH-c5-gly)]+ 32* N-[(N2-benzhydryloxycarbonylguanin-9-yl...



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0.28/5
...), 68.2 (C2), 66.1 (C3), 52.9 (C5) and 50.8 (OCH3); νmax (KBr...), 68.2 (C2), 66.1 (C3), 52.9 (C5) and 50.8 (OCH3); νmax (KBr...), 67.8 (C2), 65.9 (C3), 53.1 (C5) and 48.7 (OCH3); νmax (KBr...), 67.8 (C2), 63.9 (C3), 51.9 (C5) and 46.3 (OCH3); νmax (KBr...), 68.6 (C2), 64.4 (C3), 53.1 (C5), 50.2 (OCH3) and 21.9 (CH3... Tetrahedron (C2) 65.2 (C3), 52.4 (C5), 50.6 (OCH3) and 40.6 (CH2...), 123.5 (indole C2'), 122.3 (indole C5'), 120.8 (indole C4'), 118.9 (indole...), 67.5 (C2), 65.9 (C3), 53.1 (C5) and 48.6 (OCH3); νmax (KBr..., 1H, NH); δ (13C): 172.8 (CO), 142.1, 140.9, 137.6, 136.4, 130 (Cq...), 67.6 (C2), 64.1 (C3), 52.1 (C5) and 46.2 (OCH3); νmax (KBr... (s, 3H, CH3); δ (13C): 175.7 (CO), 142.0, 140.8, 136.5, 134.9 (Cq), 129...), 69.0 (C2), 64.9 (C3), 53.4 (C5), 50.4 (OCH3) and 22.3 (CH3... (s, 2H, CH2); δ (13C) 174.6 (CO), 142.1, 140.9, 137.1, 136.5, 135.1 (Cq...), 73.4 (C2), 65.2 (C3), 52.9 (C5) 50.8 (OCH3) and 41.0 (CH2....1 (ArOCH3), 54.0 (CO2CH3) and 52.5 (C5); νmax (KBr): cm-1; m/z (ES+): 423...), 56.1 (ArOCH3), 56.0 (CO2CH3), 52.7 (C5) and 21.4 (CH3); νmax (KBr...), 67.6 (C3), 55.5 (ArOCH3), 53.0 (C5) and 40.7 (OCH3); νmax (KBr...), 64.3 (C3), 56.7 (ArOCH3), 56.3 (C5), 53.2 (OCH3) and 21.9 (CH3...), 150.7 (furan C2'), 143.0 (furan C5') 133.1, 133.0 (Cq), 128.2, 128...), 67.1 (C2), 64.3 (C3), 52.7 (C5) and 48.2 (OCH3); νmax (KBr...), 150.1 (furan C2'), 143.1 (furan C5') 133.8, 133.5 (Cq), 128.9, 128...), 69.9 (C2), 65.8 (C3), 53.5 (C5), 51.5 (OCH3) and 22.5 (CH3...), 74.4 (C2), 66.1 (C3), 53.0 (C5), 52.3 (OCH3) and 40.8 (CH2...), 151.2 (furyl C2'), 143.4 (furyl C5'), 142.0, 140.7, 133.3 (Cq), 129.2 (2 x ArCH...), 67.9 (C2), 65.2 (C3), 53.3 (C5) and 49.3 (OCH3); νmax (NaCl...), 68.5 (C2), 67.8 (C3), 53.3 (C5) and 50.9 (OCH3); δB (1H, 300....2 B B Tetrahedron (C2), 64.9 (C3), 52.6 (C5) and 49.4 (OCH3); νmax (KBr...), 68.8 (C2), 64.4 (C3), 53.4 (C5), 52.3 (OCH3) and 22.2 (CH3...), 73.1 (C2), 64.9 (C3), 53.4 (C5), 53.0 (OCH3) and 40.9 (CH2...), 94.2 (C4), 67.6 (C3) 65.0 (C5), 53.0 (C2) and 49.1 (OCH3...), 67.6 (C2), 67.2 (C3), 53.1, (C5) and 52.4 (OCH3); νmax (KBr...), 68.8 (C2), 65.1 (C3), 54.6 (C5), 53.5 (OCH3) and 22.8 (CH3.../hexane as colourless plates, m.p. 134-142 °C. Found: C, 66.45; H, 6.50; N, 8.00...), 123.9 (ArCH), 96.3 (C4), 66.8 (C5), 64.2 (C2), 53.4 (OCH3), 45...), 67.5 (C2), 64.3 (C3), 52.9 (C5), 45.6 (OCH3), and 23.2 (CH3...), 108.5 (Cq), 90.8 (C4), 64.3 (C5), 63.3 (C2), 53.2 (OCH3), 41...), 64.3 (C2), 63.8 (C3), 53.0 (C5), 46.4 (OCH3), and 22.7 (CH3... CO), 168.5 (ester -OCO), 151.6, 142.2, 140.3, 140.0, 136.5, 129.9 (Cq....8 (Vanillin ArCH), 96.3 (C4), 66.4 (C5), 62.2 (C2), 55.9 (ArOCH3), 52...), 64.3 (C2), 63.8 (C3), 53.0 (C5), 46.4 (OCH3), and 22.7 (CH3...



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0.15/5
...)# l5 I44.93*, I43.75*, 142.49*, I41.71 *, I38.89... F NMR F NMR (CDCh, 188 MHz) c5 -134.23 (ddd, 1 = 6Hz, 12Hz...); 19 F NMR (CDCh, 188 MHz) 6-142.21 (m, 2F), -153.97 (t, 1 = 21... out. 1 H NMR (CDCh, 200 MHz) c5 5.71 (s, IH, CH0 2 ), 3.4-3.9 (m, 4H, OCH2... ); 13 1 C { H} NMR (CDCh, 100 MHz) c5 144.86 (d, 1 =250Hz, CF), 141... 3 ); 19 F NMR (CDC1 3 , 188 MHz) c5- 142.91 (m, 2F), -154.48 (t, 1 = 20... white solid, mp 182 2 3 MHz) c5 168.23, (CO), 82.96... 3 ); 19 F NMR (CDCh, 188 MHz) c5 -141.26 (s, 4F) (see appendix....69 (s, 4F) (see appendix page 142). 2.4.14 5,6,28,29,30,31...-transconfiguration. 1 lljlliljilliptiljlllljlllljlllljlllijlillllll!jlllljlllljlliijiiilJilllllllljllllllllljlltljillljllllllllljlllljl l lljlllljillljlilljlilljlllll -138 ·142 Figure 3.2.8 ·146 19 -150 -154...%; M 470. 1 HNMR (CDCh, 200 MHz) c5 4.15 (t, J =7Hz, 4H, CH20), 2.20...); 13 1 C { H} NMR (CDCI 3 , 62.9 MHz) c5 145.21 (d, J = 245Hz, CF), 140... 2); 19 F NMR (CDCh, 188 MHz) 6 -142.54 (m, 4F, CF ortho to...) o o 19F NMR (CDCh, 188 MHz) o- 142.67 (s, 4F). 3.4.8 2,3,4,5~ Tetrafluoroxylylene~ 1,4~bis(triphenylphosphonium... NMR (DMSO-d6, 300 MHz) c5 8.0-7.6 (ms, 30H, ar. CH), 5.30... C NMR (DMSO-d6, 100 MHz) c5 135.57 (ar. CH), 134...); F NMR (DMSO-d6, 188 MHz) c5 -137.26 (s, 4F) (see appendix.... 96 oc), (CDCh, 200 MHz) c5 3.77 (s, 6H, OCH3 ), 3.73 (s, 6H... shows three new resonances at b -142.11, -156.11 and -162.... 19 F NMR (C 7D 8 , 188 MHz) 6 -142.11, -143.81, -156.11... MHz) c5 7.20 (s, 4H, CH=CH); F NMR (C Ds, 7 8 7 188 MHz) c5 -142.95...]iillllllljlllljlllrjliirjiriljlllrjllll]lllijllii]rirljlllljllll(lllijllllj\llljlllljllrl] -138 -142 -146 -150 -154 -158 I ppm... -135 I I I I I I I I I -145 I I I I I I I I I -155 I I I I I I I I I I I I I I I I -165 pp m 142 5,6,28,29,30,31 ,32...-137-138-139-140.141-142-143-144-145 ppm 151... spectrum TTIIIIII''''I''' 'I' '''I''''I''''I'TTT] 1111111111''''1''''1''''1''''1''''1''''1''''1''''1''''1''''1''''1''''1' ,, '1''''1''''1''''1''''1''''1''''1 -138 -142 -146 -150 -154 -158 pp...



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0.16/5
... h; b Conversion determined by 1H NMR; c5 mol% PPh3 Table 1 - Tertiary Amine... h; b Conversion determined by 1H NMR; c5 mol% PPh3 Table 2 - Secondary Amine....4 MHz, CDCl3, 25 °C): δ = 145.9 (C6), 142.3 (C10), 128.5 (C12), 128.5 (C8... (75.4 MHz, CDCl3, 25 °C): δ = 144.4 (C5), 142.4 (C9), 118 Chapter 7 128.6 (C7....4 MHz, CDCl3, 25 °C): δ = 146.4 (C9), 142.5 (C5), 128.8 (C11), 128.4 (C6 & C7... NMR (75.4 MHz, CDCl3, 25 °C): δ = 142.3 (C5), 140.5 (C9), 128.5 (C7 & C11... C NMR (75.4 MHz, CDCl3, 25 °C): δ = 142.7 (C5), 140.1 (C9), 129.0 (C10), 128... NMR (75.4 MHz, CDCl3, 25 °C): δ = 142.6 (C5), 128.5 (C7), 127.1 (C6), 125....4 MHz, CDCl3, 25 °C): δ = 142.2 (C4), 128.5 (C6), 128.4 (C5), 125.9 (C7), 50... NMR (75.4 MHz, CDCl3, 25 °C): δ = 142.5 (C9), 128.5 (C11), 128.4 (C10..., 25 °C): δ = 152.2 (C11), 142.8 (C4), 141.9 (C8), 128.5 (C5 & C6), 126.0 (C7... (75.4 MHz, CDCl3, 25 °C): δ = 167.9 (C5), 133.3 (C1), 129.9 (C4), 129... C NMR: (CDCl3, 75.4 MHz) δ = 168.8 (C5), 134.2 (C1), 131.7 (C4), 128... °C): δ = 140.9 (C4), 128.4 (C6), 128.2 (C5), 125.9 (C7), 38.2 (C1), 31....4 MHz, DMSO-d6, 25 °C): δ = 145.8 (C5), 128.5 (C7), 126.8 (C6), 126... °C): δ = 143.9 (C4), 128.5 (C6), 127.4 (C5), 126.3 (C7), 47.2 (C3), 37... °C): δ = 157.6 (C7), 132.7 (C4), 129.2 (C5), 113.8 (C6), 55.0 (C8), 38... (75.4 MHz, DMSO-d6, 25 °C): δ = 142.1 (C10), 128.2 (C8), 128.2 (C9... (75.4 MHz, CDCl3, 25 °C): δ = 145.7 (C5), 137.7 (C9), 133.7 (C11), 132...), 137.6 (d, J = 9.3 Hz, C1), 124.5 (d, J = 3.0 Hz, C5), 117.3 (d, J = 7.2 Hz, C4), 116.2 (d, J = 21...) δ = 149.6 (C1), 131.8 (C3), 128.9 (C5), 126.4 (C2), 120.4 (C4), 115...) δ = 148.1 (C1), 138.7 (C3), 128.9 (C5), 116.3 (C4), 112.3 (C2), 108...) δ = 148.8 (C1), 134.9 (C3), 129.9 (C5), 115.1 (C4), 111.4 (C2), 109...), 131.5 (d, J = 31.4 Hz, C3), 129.6 (C5), 124.8 (d, J = 272.1 Hz, C9), 114... consistent with literature data.31 142 Chapter 7 4-(3-Phenylpropyl)morpholine 4.15 According...: (CDCl3, 75.4 MHz) δ = 142.2 (C4), 128.5 (C6), 128.4 (C5), 125.9 (C7), 67...); 13C NMR: (CDCl3, 75.4 MHz) δ = 142.5 (C5), 128.4 (C7), 127.5 (C8), 126...); 13C NMR: (CDCl3, 75.4 MHz) δ = 142.6 (C6), 128.4 (C8), 127.5 (C9...: (CDCl3, 75.4 MHz) δ = 142.5 (C3), 128.4 13 (C5), 127.5 (C6), 126.0 (C4...); C NMR: (CDCl3, 75.4 MHz) δ = 13 142.0 (C5), 128.5 (C7), 127.7 (C8), 126...: (CDCl3, 75.4 MHz) δ = 13 142.3 (C9), 138.2 (C5), 129.2 (C11), 128.5 (C6..., 75.4 MHz) δ = 145.7 (C9), 140.2 (C5), 128.8 (C12), 128.5 (C7), 128...) and isolated as a yellow oil (142 mg, 80%). 1H NMR: (CDCl3...) δ = 167.6 (C1), 135.0 (C2), 131.4 (C5), 128.6 (C4), 127.0 (C3), 40..., 75.4 MHz) δ = 163.1 (d, J = 245.4 Hz, C5), 148.7 (d, J = 6.6 Hz, C3), 130.1 (d, J = 8.1 Hz...: (CDCl3, 75.4 MHz) δ = 143.5 (C6), 142.9 (C5), 139.5 (C3), 118.6 (C8), 117....4 MHz) δ = 162.1 (d, J = 244.7 Hz, C6), 142.4 (d, J = 7.1 Hz, C4), 139.1 (d, J = 3.0 Hz, C3....0 (d, J = 8.4 Hz, C8), 115.8 (d, J = 23.0 Hz, C5), 113.1 (d, J = 20.9 Hz, C7), 65....2 (C4), 143.8 (d, J = 1.1 Hz, C3), 130.0 (C5), 128.8 (d, J = 32.3 Hz, C7), 124..., 75.4 MHz) δ = 161.2 (d, J = 243.6 Hz, C5), 145.8 (d, J = 3.8 Hz, C3), 127.4 (d, J = 15...); 13 C NMR: (CDCl3, 75.4 MHz) δ = 142.6 (C5), 141.0 (C6), 136.6 (C3), 129...) δ = 140.0 (C3), 134.6 (C4), 133.4 (C5), 131.9 (C10), 128.8 (C9), 127...); 13C NMR: (CDCl3, 75.4 MHz) δ = 142.6 (C7), 139.1 (C8), 129.1 (C10...) δ = 170 Chapter 7 143.3 (C3), 136.1 (C5), 136.0 (C8), 129.6 (C7), 128....4 (C8), 140.9 & 140.7 (C3), 135.5 (C5), 128.1 & 128.1 (C4), 126.1 & 125...) δ = 208.2 (C1), 142.1 (C3), 138.0 (C4), 128.8 (C6), 126.9 (C5), 46.7 (C8....4 MHz) δ = 208.4 (C2), 142.4 (C3), 138.1 (C9), 132.2 (C5), 128.7 172 Chapter...) δ = 202.2 (C1), 142.2 (C11), 139.0 (C3), 138.0 (C8), 135.6 (C5), 132.3 (C6....4 (C1), 176 Chapter 7 142.9 (C3), 137.5 (C8), 135.0 (C5), 132.3 (C6), 130...), 138.4 (d, J = 3.1 Hz, C4), 128.2 (d, J = 8.1 Hz, C5), 115.5 (d, J = 21.4 Hz, C6), 115..., C8), 146.9 (C2), 137.8 (d, J = 3.1 Hz, C5), 128.3 (d, J = 8.1 Hz, C7), 115.3 (d, J = 21...), 70.1 (C1), 17.4 (C4), 13.4 (C5); Minor 162.2 (d, J = 244.6 Hz, C9....2 (d, J = 8.1 Hz, C9), 128.1 (C2), 126.8 (C5), 115.6 (d, J = 21.4 Hz, C10), 74....3 (d, J = 245.0 Hz, C8), 139.7 (d, J = 3.1 Hz, C5), 134.3 (C3), 127.6 (d, J = 8.1 Hz, C6..., H7), 139.4 (C2), 138.0 (d, J = 7.8 Hz, C5), 136.3 (d, J = 3.1 Hz, C4), 127.8 (d, J = 8.5 Hz...), 138.1 (d, J = 3.5 Hz, C4), 129.6 (d, J = 5.3 Hz, C5), 125.4 (d, J = 8.1 Hz, C9), 125.1 (d, J = 17....7 (C2), 139.6 (d, J = 3.8 Hz, C4), 128.7 (C5), 126.2 (d, J = 7.2 Hz, C9), 121.1 (d, J = 17...), 116.2 (C3), 115.4 (d, J = 17.8 Hz, C5), 74.3 (d, J = 1.3 Hz, C1); 19F NMR...), 125.2 (qd, J = 4.6 1.7 Hz, C9), 124.5 (C5), 122.7 (q, J = 272.0 Hz, C10), 118...), 129.4 (d, J = 8.3 Hz, C7), 127.8 (d, J = 4.2 Hz, C5), 124.5 (d, J = 3.5 Hz, C6), 115.6 (d, J = 21...) δ = 199.2 (C1), 151.0 (C7), 130.4 (C5), 124.6 (C4), 110.8 (C6), 47...) δ = 199.3 (C1), 154.5 (C7), 130.2 (C5), 126.5 (C4), 113.5 (C6), 48...) δ = 199.1 (C1), 152.3 (C7), 130.6 (C5), 124.5 (C4), 110.2 (C6), 49...) δ = 202.1 (C1), 152.9 (C7), 141.7 (C5), 131.7 (C9), 127.8 (C4), 117....5 (d, J = 3.2 Hz, C8), 116.0 (d, J = 21.9 Hz, C5), 66.9 (C11), 50.3 (d, J = 4.4 Hz, C10....6 (C9), 132.5 (C4), 128.2 (q, J = 5.4 Hz, C5), 125.8 (d, J = 29.6 Hz, C6), 123...



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1.91/5
...-1,3-пентадиена с заданными молекулярными характеристиками» C1-142 C. А. Романов, С. Ю. Ердяков, М. Е. Гурский, Е.С.Гарина, М.Ю. Заремский... и их молекулярных масс турбореометрическим методом» C5-142 Д.А. Маркелов, Ю.Я. Готлиб «Зависимость механических свойств..., C. Plesse, D. Teyssié, C. Chevrot, Synthetic Metals, 142, (2004 )287. 3. F. Vidal, C. Plesse, G. Palaprat... Президиума РАН "Поддержка инноваций и разработок". 142 Секция 2 Устные доклады Акриловые сополимеры..., С5204 Алешин В.В. C3-3 Алиев Л.П. C5-8 Алиев М.А. C5-3, C5-4 Алиновская В.А. C1-197, C2-57..., 276, C4-79, C5-7, C5-81, C5205,C5-207, C5-268 Бакеева И.В. C4-9, C4..., C5-115, C5143 Балабанова Ф.Б. C1-70 Балакин В.М. C1-11, C5187 Балакин К.В. 142 Балакина М.Ю. C3-7, C329, C3-103 Балашов В.А. C1-12, C5-15 Бандурян С.И. C5..., C2-54, C2-55 Бачурин С.О. 142 Баяхметова З.К. C3-77 Беганцова Ю.Е. C3... Бубнов М.П. C1-192 Бубнов Ю.Н. C1-142 Бубнова Л.И. 184 Бугаенко М.Г. 100 Бугаков..., C1177, C4-29, C5-32, C5-33, C5-42, C5-46, C5-166, C5167 Бузинова... Е.В. C5-41 Бурда В.В. C5-27, C5-249 Бурдуковский В.Ф. 108 Бурмистров В.А. C5-22 Бурова Т.В. 254, C5..., C4-79, C5-7, C581, C5-205, C5-207, C5-238, C5-239, C5-268 Вольфсон С.И. C1... О.В. 240 Вялова А.Н. C5-51 Габдрахманов Д.Р. C5-52, C5-53 Габитов И.Т. C1-7, C5-9 Габриелян Г.А. C2... Ганев В. C5-43 Ганина Л.В. C5-56 Ганифаева Н.А. C5-8 Гаппарова Г.И. C1-138, C5-57, C5-58 Гараева Г.Ф. C1-33 Гарина Е.С. C1-76, C1-142, C1-152, C1-195, C5-100 Гарифуллин Д.Ш. C1-11 Гаришин О.К. C5-59..., C5-60 Гегель Н.О. C5-257 Ген Д.Е. 243 Герасименко С.А. C5-61 Герасимов В.И. C5-181, C5-205 Герасимов Р.А. C5-62 Герасин В.А. 190, C1-5, C219, C5-59, C5-63, C5..., C1-76, C1-195, C1-142, C1-143, C1178, C3-17...-96, C1-152, C5-210 Готлиб Ю.Я. 220, C5-74, C5-142 Гофман И.В. 234, C3... В.Я. 254, C5-36, C5-75, C5-84 Гринберг Н.В. 254, C5-36, C5-75, C5-84 Грингольц..., C4-12 Гурский М.Е. C1-142 Гусарова Е.Б. C5-104 Гусев А.В. 244 Гусев К.И. C4..., C2-19, C5-59, C5-63, C5-78 Гуткович С.А. C5-79 Даванков В.А. C5-178 Давиденко... П.В. 246, C580, C5-224 Добровольская И.П. 234, C5-83, C5-191 Добрун Л.А. C5-134 Добрусина... А.В. C4-9 Долгих О.В. C5-158 Долгов В.В. 201 Долгова А.А. C5-7, C5-81 Долгоносова А.М. C5-259 Долгополов...-43 Дубовик А.С. 254, C5-36, C5-75, C5-84 Дубовицкий В.А. C5-48 Дубровский В.В. C4..., C1187, C3-49, C5-107 Ердяков С.Ю. C1-142 Еремина Т.В. C1-51 Ермак... О.Е. C5-231 Запуниди С.А. C3-36 Заремский М.Ю. C1-19, C1-76, C1-142..., C3115, C3-51, C5-118, C5-139, C5-145, C5-151, C5-164, C5200 Иванов...-52 Иванов Р.В. 130, 142, C375 Иванова А.В. C5-97 Иванова В.О. C5-38, C5131 Иванова... Р.С. C1-105 Кожунова Е.Ю. C5-108, C5-169 Козлов А.В. C5-109, C5-231 Козлов В.В. C1...-33, C4-86, C5-133, C5-157, C5-204 Косточко А.В. C5-40, C5135 Костюк...-77, C5-5, C5-205 Курмаз С.В. C1-117, C4-57, C5-101, C5-125, C5-197...-28, C4-29 Лозинский В.И. 130, 142, C2-15, C2-38, C3..., C1177 Макарова Е.Н. C5-56 Макарова Л.И. C5-46, C5166, C5-32 Макарова М.А. C5-47 Маковецкий..., C5-130 Марк С. 105 Маркелов Д.А. C5-142, C5143 Маркин А.В. 209, C5-93, C5-144, C5-208...-163 Масленникова Т.П. C5-83, C5-191 Мастюгин А.В. C5-189 Матвеев В.К. C5-240 Матвеева И.А. C4... Н.Г. C5-38, C5131, C5-132 Матнишян А.А. 270 Матусевич Ю.И. C5-87, C5-263 Матухин Е.Л. C5-40... В.С. 229, 242, 284, C5-155, C5-184, C5-253 Молькин В.Е. C5-186 Монаков Ю.Б. 97... Морозов П.В. C5-156 Москалев И.В. C5-47 Москаленко Ю.Е. C5-150 Москвин Ю.Л. C5-160 Москвина М.А. C5-238..., C4-79, C5-6, C5-109, C5140, C5-160, C5-185, C5208, C5-241 Мукменева Н.А. C3...-67 Никулова У.В. C5-168 Нилов Д.Ю. C5-217 Нистратов А.В. C5-77, C5106, C5-196 Нифантьев...-155, C5-77, C5106, C5-170, C5-171, C5183, C5-192, C5-196 Новакова А.А. C5-169..., C1-177, C5-32, C5-33, C5-36, C5-42, C5-166, C5-248 Паращук Д.Ю. C3... Романов C.А. - C1-142, C1143 Романов Г.А. - C5-44 Ронова И.А. 226, C5-204, C5-219 Рощупкин..., C5-161 Смирнова Л.Г. C5-214 Смирнова Н.М. 136 Смирнова Н.Н. C5-127, C5-144, C5-208, C5-215... Н.П. C4-4 Солдатов В.С. C5-220 Соловова Ю.В. C5-262 Соловская Н.А. C5-223 Соловцова О.В. C5-221 Соловьев... М.В. 177 Тарабукина Е.Б. 228, C5-6, C5-109, C5-231 Тарасевич К. C5-3 Тарасов А.Е. C1-169 Тарасюк...-15 Темнов Д.Э. 247, C5-27, C5-232, C5-243, C5-244 Тепляков В.В. C3-56... Филиппов A.П. 103, 228, 269, C5-6, C5-109, C5-212, C5-231 Филиппов А.Н. C1-178..., C1-13, C2-3, C5-119, C5-120, C5-155, C5-184 Финкельштейн Е.Ш. 106, C1...-14, C5-30, C5-31, C5-66, C5126, C5-168, C5-182, C5193, C5-222 Чапурина..., C5-80, C5-113, C5140, C5-156, C5-191, C5224, C5-235, C5-264 Челушкин П.С. C5-76, C5100, C5-138 Червинский Т.И. C1-193 Червятина М.Е. C5... В. C5-254, C5-255 Шилова И.А. C5-256 Шилова С.В. C3-10 Шинкарев С.М. C5-221 Шипина О.Т. C5... Л.М. 250, 276, C5-7, C5-81, C5-205, C5207, C5-268 Ясина Л.Л. C5-43, C5-138 Ясногородская...



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0.15/5
... 116/C2 116/A3 115/C5 095/B8 095/C1 087... 220/A4 078/A3 077/C5 078/A4 077/C7 078... 060/C3 060/C4 060/C5 060/C2 060/C7 061... 144/C8; 145/A1144/C5 045/C5 045/C6 6897 6900 4357.../Fisch 051/B5 051/C2-C5 051/B2-B4 051/B1... 104/B4 104/B6 103/C5-C8 103/C1-C3 Catalog...; C1 099/C2 099/C3-C5 099/C6 099/B7 099.../B8; Cl 3143a 102/C2-C5 102/C6 102/A6-A7.../A5 058/A3-A4 042/C5 219/C5 219/C6 3132 3115... 235/C2 235/C3 235/C5 235/C4 235/C6 235/C7 235/C8 215/C5 215/C6 215/C7 215...-C7 125/B7-B8 125/C5-C6 1768 1772 1766 1767... 6273 6272 1.93/C6 193/C5 193/C7 193/C4 193.../C3-C4 218/C1 180/C5 3778 3762a 3762b 127/A1... 194/B6-B7 194/C3-C5 194/B5 3752 6283 5738... 185/C6 185/C7 185/C5 189/C7 189/C8 190.../C2 181/C8 181/C5-C7 197/C4-C5 198/A7 197... 177/C1 177/C3 192/C5 192/C8 193/A5 193... 184/C6 184/C4 184/C5 6057 6048 6060 6060a 6060b... 5982 5958 186/B8 186/C5 186/A3 186/B1-B2.../A3-A6__ 178/C4 178/C5-C6 178/C7-C8 5666... 181/B5 192/A7 191/C5 192/A5 191/C6 191.../A7-A8; B1 177/C4-C5 5635 5633 5634 5726 5729... 199/C8 199/C7 198/C5 183/B8 199/C2 199/C3 199/C1 Catalog _ _ 218/C5 218/C6 192/C3 176... 175/C7-C8 175/C3-C5 6485a 6483 6937 6938 6228.../C8 190/C2-C3 190/C5 6258 6253 6255 6503 6502... 176/C2-C3 176/C4-C5 6161 6162 6150 6160 5624... 188/B2-B4 188/C4-C5 6072a 6072b 6068 6071 6074.../C6-C7 075/C4 232/C5 105/C5 106/A3 105/A7... Frame/Fisch Catalog 4677 1531C3-C5 153/C6-C7 153/C8... 4519a 148/Al 4533 147/C5 148/A2 147/C8 147... 146/C7 146/C8 146/C5-C6 4521 4534 4532 4520...-B5 209/A3-A4 212/C5 2121C6 207/B4-B5 215.../A3-A4 013/C4 013/C5 0364a 013/C6 013/C7...-B 0400c 014/C6-C8 015/C5 399 413 015/B8; Cl... 016/Al 015/C4 014/C5 015/C2 015/C7 015... 2801 Frame/Fisch 094/C4-C5 094/C7-C8 094/B8.../B6-B7 049/C4 049/C5-C6 Catalog Familia Ericaceae Ericaceae...-B3 095/A1-A3 093/C5-C8; 094/ 094/A2-A3.../A6-A7 109/A6 109/C5 2976 2981 2972 2972a 2971... 220/B4 220/C4 220/C5 220/C6 221/C7 220... 768 035/C8_ 035/C3-C5 035/C6-C7 235/A7...; Cl 020/C2-C4 020/C5 020/84 020/B3 023... 023/B2-B4 nutans 022/C5-C8; 023// praecox 0548a 023/A3 praecox 021/C4-C5 subspicata 0542b 022/A1-A3.... M.Thunb. 234/A5 barbatum 233/C5 distachyum 233/C8 hirtum 234... Frame/Fisch 031/C2 031/C5-C6 031/C7 031/C8... 0636a 030/C6-C7 030/C5 0620a 029/B5-B6 029... 029/C3-C4 0622a 029/C5 0624d 030/A8 030/C3... 026/C7 026/C4 026/C5 442 599 598 0598a 596.../C8 234/C2-C3 234/C5-C6 234/C4 7332a 234... 645 031/86 682 032/C5-C8; 033/) 681 032/C4... 457 zizanoides (Andropogon muricat 016/C5 Species murinum murinum murinum (rigidum... 034/B7 034/B8 034/C5-C6 034/C8 0571a 035... floridanum officinalis Frame/Fisch 206/C5-C6 058/B4-B7 6827...; Cl 1579a 058/C2 058/C5-C6 058/C3 058/C4 124/B5 174/C4 174/C5 1584 1580 1582 3725 5558.../A7 059/C8 059/C4-C5 059/C6-C7 _ 2428-_ 2434... 084/C6 2483d 084/C3-C5 082/A5 084/C1-C2... 082/C3 082/C4 082/C5-C8 2477 2471 2471a 2471b... 135/A7 4067 138/C4-C5 4033 136/A6-A8 4032.../C8; 138/A14053 137/C4-C5 4059, 137/C8 134/A8... 176 4022 4023 1351C4__ 135/C5 135/C6-C7 135/C3...-C 4018a 4181 141/C2 141/C5-C6 141/C3 141/68... 139/C5-C7 139/C8 139/C3 139/C4 142/A8 142/A4 142...-B7 008/C2-C4 008/C5-C7 008/81 0193a 195... 4042 4039 4040 1421A1 142/A3 141/C7 142/A2 136/B8.../C6 136/C2-C4 136/C5 139/A2 4083a 4083 4094.../A3-A5__ 139/A6 134/C5-C7 134/C8 134/6465...-C 135/Al 135/A2 140/C5 140/C6 141/Al-A2... 170/A2 092/B8 170/C5 092/C2 5404a 2846 5438.../A8 5341 5321 168/C3-C5 169/B8 5301 5377 169... 238/A8 237/C5 237/C6-C7 163/C5 165/A8 165... 075/B8 074/C4 074/C5 2150a 075/B6-B7 2151b.../B5 160/C4 4877a 160/C5-C6 160/C7 161/B4... 3478a 110/C4 110/C5-C6 110/C5-C6 224/C6-C7... 7464b 238/C3-C6 002/C5 002/C6-C7 0043a 003.../Fisch 202/C7 6652a 202/C5 146/A2 146/A3 146...; B1 B1 204/A4 204/C5 204/C6-C8 6732a 203.../Fisch 039/C3 039/C4-C5 039/B4-B8; C1-C 041.../A3-A4 0908b 040/C4-C5 0914a 040/C6-C7 040... 223/A1-A3 7011 a 222/C5 074/C1 074/C1 2128a... 2820a 091/C3-C4 091/C5-C6 086/A3-A4 086...-B7 085/B8 2514a 085/C5 086/A7-A8; B1-B; B1.../A3-A4 047/C3 047/C5 047/C6 1112a 11 12a... 112/C2-C3 112/C4-C5 112/C6-C8 Catalog 3645... 111/C4 3489a 3489b 111/C5-C6 115/C3 115/C4... 116/C8; 116/C4 116/C5 117/A2 3588a 117/A3...-A8;131-1 B1-B: 3: 037/C3-C5 038/C3-C6 038/C7... 7141c 227/A8 7141d 228/C5 228/B4-B7 7147a 7147b.../C7-C8; 231/> 230/C4-C5 7157a 7157C 231/A2-A4... 229/C2-C4 7153b 229/C5-C7 7153e 7153c 1657 1356.../B6-B7 7156b 227/C4-C5 7130a 225/A6 225/A7.../A8 7130c 7130e 225/C4-C5 7130i 7130Î 225/B2-B3... 301 5a 3015a 0951C5 095/C5 096/C5-C6 096/A3-A6... 301 9a 096/B3 098/C5 3048a 098/C6-C7 3048c.../A5 143/81-B2 142/B1-B2 142/B3 007/B4-B5.../81 144/B2 144/A8 142/C7 142/C8 143/C7 144.../C3 144/B3 145/C5 142/B4-B5 142/B7 4301 4308 4303... 145/C3 142/B6 142/C2-C3 142/C4 142/C6 142/C5 142/B8 142/C1 041.../B7 005/C3-C4 005/C5 0918a 4332 4337 4331 4339... 006/B6 007/A6 231/C5 china? 232/Al excelsa herbacea...-C3 089/C6-C8 089/C5 089/C4 127/A8 3310a... Frame/Fisch 063/C7 063/C5-C6 071/C3-C6 069... 065/C8 065/C7 065/C5-C6 Catalog 1792g 1792f 2042...-B2 070/A6-A8 068/C5 068/C6 068/C4 - 1987...-C8; 071// 071/B6 070/C5-C6 071/B3-B5 071... 007/C8 007/C6 007/C5 007/C4 007/C7 2019... 201/Al 200/C4 200/C5 200/C8 200/C7 1902.../Fisch 241/C2-C4 241/C5 241/C6-C8 241/A8... 7763b 7763c 246/A2 245/C5 246/A3 245/C4 245... 265/C4 265/B3 265/C5-C6 265/B4 8063 8077... san uineus Pagina 73 267/C5 267/C1 267/C4 267...